By Reece H Vallance

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1998). , 1998). 0% HO (69) O OH O (68) (35) Fig. 21. Ultrasound-catalysed synthesis of Knoevenagel reaction product (68). , 2011). , 2011). 0% O H3O+ O (70) Fig. 22. Synthesis of coumarinic compound (70) with and without ultrasound irradiation. 7 Solvent-free Knoevenagel reactions As mentioned previously, the reduction or elimination of volatile organic solvents in organic syntheses is one of the main goals in green chemistry. Solvent-free organic reactions result in syntheses that are simpler and less energy-intensive, and these conditions also reduce or eliminate solvent waste, hazards, and toxicity (Tanaka, 2003).

0% (49) (48) Fig. 13. Compound (48) synthesis. , 2006). In the pharmaceutical industry, companies are using biotechnology to develop 901 medicines and vaccines targeting more than 100 diseases (Castellani, 2001a). In 2010, 26 new treatments were approved, and five of these treatments were based on biotechnology (Castellani, 2001b). 0% when the reaction was catalysed by alkaline protease from Bacillus licheniformis (BLAP) in a DMSO:H2O (9:1) solvent at a temperature of 550C (Fig. , 2011). 0% (44) Fig.

De Oliveira, V. & Menegatti, R. (2011). Condensation of Ethyl Cyanoacetate with Aromatic Aldehydes in Water,Catalyzed by Morpholine. 1, (January 2011), pp. , Arvanitis, E. , Pottorf, R. S. & Player, M. P. (2003). Solid-Phase Synthesis of a Tyrphostin Ether Library. 4, (January 2011), pp. 408-413, ISSN 1520-4766 Hajipour, A. R. & Rafiee, F. (2010). Acidic Bronsted Ionic Liquids. 4, (July 2010), pp. 285-362, ISSN 0030-4948 Hangarge, R. , Jarikote, D. V. & Shingare, M. S. (2002). Knoevenagel condensation reactions in an ionic liquid.

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