By Joseph A. Vinson

ISBN-10: 0841204888

ISBN-13: 9780841204881

ISBN-10: 0841206287

ISBN-13: 9780841206281

content material: A survey of metabolic variations of [delta]¹-tetrahydrocannabinol / Sumner Burstein --
GLC and HPLC analyses of cannabinoids in organic fluids and functions / E.R. Garrett, A.J. Gouyette, and C.A. Hunt --
Detection and quantitation of tetrahydrocannabinol in physiological fluids / Monroe E. Wall, Dolores R. Brine, Joan T. Bursey, and David Rosenthal --
Quantitation of [delta]⁹-tetrahydrocannabinol and 11-nor-[delta]⁹-tetrahydrocannabinol-9-carboxylic acid in physique fluids by means of GC/CI-MS / R.L. Foltz, P.A. Clarke, B.J. Hidy, D.C.K. Lin, A.P. Graffeo, and B.A. Petersen --
development of the mass fragmentographic strategy for quantification of tetrahydrocannabinol in human blood plasma / Agneta Ohlsson, Stig Agurell, Jan-Erik Lindgren, and Kurt Leander --
A basic method of the research of cannabinoids from physiological resources / J. Rosenfeld --
Quantitation of [delta]⁹-tetrahydrocannabinol and its metabolites in human urine by means of likelihood established matching GC/MS / Donald E. eco-friendly, Fu-Chuan Chao, Kay O. Loeffler, and Saul L. Kanter --
HPLC research of [delta]⁹-tetrahydrocannabinol and metabolites in organic fluids / Seth R. Abbott, John R. Berg, Kay O. Loeffler, Saul Kanter, Leo E. Hollister, Joan Hawkins Abrams, Hugh L. Baras, and Reese T. Jones --
Radioimmunoassay of cannabinoid compounds / C.E. cook dinner --
Antisera raised opposed to tetrahydrocannabinol within the radioimmunoassay of cannabinoids / J.D. Teale, Jacqueline M. Clough, L.J. King, V. Marks, P.L. Williams, and A.C. Moffat --
HPLC analyses of [delta]⁹-tetrahydrocannabinol and 11-nor-[delta]⁹-tetrahydrocannabinol-9-carboxylic acid in human plasma / Jimmie L. Valentine, Owen H.M. Gan, H.C. Nio, and Everett D. Thompson --
Detection and quantitation of [delta]⁹-tetrahydrocannabinol in plasma by means of dansylation and double labeling / J.M. Scherrmann, R. Bourdon, H. Hoellinger, Nguyen-Hoang Nam, and E. Fournier.

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R . , Gouyette, A . , J. Pharm. , submitted (1977). G a r r e t t , E . R . , and Hunt, C. Α . , J. Pharm. Sci. 62, 1211 (1973). G a r r e t t , E . R . , and Tsau, T . , J. Pharm. Sci. 63, 1563 (1974). McCallum, Ν. , J. Chromatogr. 11, 509 (1973). McCallum, Ν. Κ . , Yagen, Β . , Levy, S . , and Mechoulam, R . , Experientia 31, 520 (1975). , Agurell, S . , L i n d g r e n , J. E . , Biochem. Pharmacol. 23, 163 (1974). Fetterman, R. S . , and Turner, C . , J. Pharm. Sci. 61, 147 Turner, C . , 62, 251 and 1083 (1973).

Several aspects of our r e s u l t s merit f u r t h e r discussion. 9 9 9 9 Choice o f Instrument Two c o m p l e t e l y e t e r s c o u p l e d w i t h d i f f e r e n t means f o r q u a n t i t a t i o n o f d a t a were u t i l i z e d . One was a r e l a t i v e l y o l d (1968) m a g n e t i c s e c t o r MS, t h e LKB-9000, w h i c h was c o u p l e d w i t h an a c c e l e r a t i n g v o l t a g e a l t e r n a t o r w h i c h p e r m i t t e d measurement o f t h e r a t i o o f t h e peak h e i g h t o f t h e unknown as compared w i t h t h a t o f t h e i n t e r n a l s t a n d a r d .

2. GARRETT E T AL. GLC and HPLC Analyses 27 same as f o r p u r i f i e d a u t h e n t i c m a t e r i a l s . 18 minutes was done by GC-mass spectrometry. Equili­ b r i a c o u l d t h e n be p o s t u l a t e d among Δ^-tetrahydrocann a b i n o l 1, c a n n a b i d i o l 10, 6,12-dihydro-6-hydroxycann a b i d i o l 8_ and p o s s i b l y ~ T s o c a n n a b i d i o l 9^ (Scheme I) . 3%) t o d e g r a d a t i o n under t h e same c o n d i t i o n s and a s s a y i n g t h e r e s u l t a n t p r o d u c t s by GLC ( T a b l e 3 ) .

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